基于贵金属-zno纳米棒的固相微萃取-表面增强拉曼光谱联用技术-分析化学专业论文.docxVIP

优秀毕业论文 精品参考文献资料 I【 I【J东大学硕士学位论文 参考文献 ．38 第三章不锈钢丝负载金．氧化锌纳米棒用于自清洁的固相微萃取-表面增强拉曼 光谱 ．．42 3．1引言 一42 3．2实验部分 ．．43 3．2．1实验试剂 43 3．2．2固相微萃取．表面增强拉曼丝的制备 43 3．2．3样品表征和SERS检测 44 3．2．4固相微萃取纤维的自清洁循环 44 3．3实验结果与讨论 一45 3．3．1固相微萃取纤维的制备和表征 45 3．3．2 SERS活性的固相微萃取纤维的均匀性 ．．49 3．3．3结晶紫和孔雀石绿的SPME—SERS联用检测 49 3．3．4水产养殖水中结晶紫和孔雀石绿的检测 55 3．3．5 SERS活性的固相微萃取纤维的自清洁性研究 ．．55 3．4本章小结 一57 参考文献 ．59 第四章全文总结 ‰ ．“ 4．1本论文创新点 ．．66 4．2有待研究的问题 一66 致谢 67 攻读硕士期间发表的论文 68 万方数据 山东大学硕士学位论文CATALoG 山东大学硕士学位论文 CATALoG Chinese abstract 。 I ABSTRACT III symboI and abbreViations ．． ． 。． V Chapter 1．Introduction ．1 1．1 IIltroduction ofR锄an spec仃oscopy ．．1 1．2 IIl仃oduction of SurfIace enhanced Raman spectroscopy ．．1 1．2．1 The basic principle ofSERS 一2 1．2．2 Memod of fabrication of SERS substmtes ．3 1．3 The application of SERS ．．9 1．3．1 Application ofSERS in enViromIlent detection ．．9 1．3．2 Application of SERS in food safety detection 11 1．3．3 SERS hyphenated teclulology ．12 1．4 Solid phase microex眦tion ．12 1．4．1 OVe州ew ofs01id phase microextraction 12 1．4。2 SPME coating ex订action mechallism硼d research progress ．1 2 1．4．3 SPME hyphenated tecll】∞logy 1 3 1．5 Background of this research and topic basis 1 7 R-efbrences ．1 8 Chapter 2 Ag-Zno nanorod arrays Via self-assembly for 3D soIid phase microextraction-surface enhanced Raman spectroscopy detection of thiram 27 2．1 IIltroduction ．27 2．2 Experimental section ．．29 2．2．1 Chemicals and instmInents ．．29 2．2．2 Preparation ofthe SERS-actiVe SPME fmer 29 2．2．3 Ch越acterization techIliques and SERS detection ．30 2．3 I沁sults aIld discussion ．30 2．3．1 Fabrication and chauraCterization ofthe Ag—Zn0 naIlorods ．．30 2．3．2 Stability and Unifo衄ity oftlle Ag-ZnO nanorods ．32 2．3．3 111e e圩ect ofextraction time ．．33 2．3．3 Q谳itatiVe and quantitatiVe SERs dete“on ofthir锄 34 2．4 ConcluSions ．．37 万方数据 lI lI I东大学硕士学位论文 Ref．erences ．38 Chapter 3 Au—coated Zno nanorods on stainless steeI fiber for self．cleaning solid phase microextraction-suI’f．ace enhanced Raman spectroscopy ·42 3．1