化妆品乳液中防腐剂测定能力验证研究-食品安全质量检测学报.PDF

7 3 Vol. 7 No. 3 2016 3 Journal of Food Safety and Quality Mar. , 2016 钮正睿, 张隆龙, 赵 阳, 张庆生, 曹 进* (, 100050) 摘 要: 目的 , , 方法 , , Z , 结果 P 0.05 , 3 , 64 , 39 , 61%结论 , 关键词: ; ; ; ; Proficiency testing on the determination of preservatives in cosmetic emulsion * NIU Zheng-Rui, ZHANG Long-Long, ZHAO Yang, ZHANG Qing-Sheng, CAO Jin (National Institutes for Food and Drug Control , Beijing 100050, China) ABSTRACT: Objective To design, conduct and evaluate the results obtained from the proficiency testing program for determination of preservatives in cosmetic emulsion, so as to assess the proficiency of the laboratories, and improve the detection and quality control capability of participant laboratories. Methods The split-level test samples were prepared for this program. Statistic analysis was performed on the determination results of methylparaben and ethylparaben, and the testing proficiency was evaluated by Z-score. The technical analysis was conducted for outlier results. Results The samples were homogeneous and stable in at least three months period at P 0.05 level, which met the requirement of PT program. A total of 39 labs which participated in this program obtained