课件：AgilentGC7890进样口简介.ppt

* * To avoid peak broadening due to the long sample transfer time, the GC oven temperature is held below the boiling point of the sample solvent during the purge delay. This causes the sample to focus at the head of the column to insure sharp capillary peaks. Note: Here we could show an inset of “Solvent Effect.MOV - this clip shows solvent and one sample component condensing at the head of the column. For this presentation it would be better to show solvent and THREE sample components entering the column, with the sample components different colors. * * Right now, we have some improvements on the design of S/SL retainer weldment nut. It is called as twist top which has very similar feature with that of current flip top. Also please be noticed that the inlet tubing is routed on the RIGHT side on the new GC. The most important thing is we only need about 1/8 turn by HAND to seal or loose the liner “O” ring. Hence it is very convenient for us to replace the liner within very short time. No longer worry about breaking the liner or burning the hands during the inlet maintenance. * * * * Agilent GC 7890进样口简介 . * 据美国化学杂志统计:95%的色谱问题是由色谱柱和进样系统造成的 Agilent GC 7890 气相色谱进样口 Agilent GC 7890 系列 进样口基本结构 进样口类型 进样方式及进样过程 进样口日常维护 Agilent GC 7890系列进样口 进样垫 衬管 衬管 O-圈 镀金密封垫 毛细管柱 Agilent GC 7890 进样口基本结构 分流/不分流进样口 (SSI) 隔垫吹扫填充柱进样口 (PPI) 程序升温冷柱头进样口(Cool On-Column) 程序升温汽化进样口 (PTV) 挥发性物质进样接口 (Volatiles Interface) 阀与气路控制系统结合，形成的阀进样系统 - 进样口类型 Agilent 7890进样口类型 Agilent 7890 GC 进样口进样方式 30ml 1.0ml 0ml 1.0ml 34ml 4.0ml 3.0ml 3.0ml 分流(Split)模式 不分流(Splitless)模式 * * * * * * * FLOW SENSOR PROPORTIONAL VALVE 1 PRESSURE SENSOR SEPTUM PURGE REGULATOR FIXED @ 3ML/MIN PURGE VALVE CLOSED FORWARD PRESSURE CONTROL LOOP GOLD SEAL INPUT PRESSURE PROPORTIONAL VALVE 2 80 PSI 5 ML/MIN SPLIT VENT TRAP 10 PSI SPLIT VENT 0 ML/MIN COLUMN FLOW 2 ML/MIN 7890 开始进样无分流动画 FLOW SENSOR PROPORTIONAL VALVE 1 PRESSURE SENSOR SEPTUM PURGE REGULATOR FIXED @ 3ML/MIN PURGE VALVE CLOSED FORWARD PRESSURE CONTROL LOOP GOLD