介孔炭制备参数对其介观结构的影响探究.pdfVIP

４７ ２ Vol．４７ No．２ ２０１８ ２ Applied Chemical Industry Feb．２０１８ １，２ １，２ １，２ ３ ４ １，２ ， ， ， ， ， （１． ， ２１００９８ ；２． ， ２１００９８ ；３．， ２１００９８ ；４．， ２１００９８） ：，、 。 ，１．０ h ，，； １．０∶１．０ ，，； １．０ h，１．０∶１．０ ，P１２３ F１２７ ， ，。 ：；；； ：TQ ４２４ ：A ：１６７１ －３２０６（２０１８）０２ －０２３８ －０５ １，２ １，２ １，２ ３ ４ １，２ ZHANG Di ，DING Ying ，JI Hui ，ZHU Xiao-hua ，YAO Huai-zhu ，ZHU Jian-zhong （１．Key Laboratory for Integrated Regulation and Resource Development on Shallow Lake of Ministry of Education， Hohai University，Nanjing ２１００９８，China；２．College of Environment，Hohai University，Nanjing ２１００９８，China； ３．Water Conservancy Department of Jiangsu Province，Nanjing ２１００９８，China； ４．Rural Water Conservancy Science and Technology Development Center of Jiangsu Province，Nanjing ２１００９８，China） ：Using the soft template synthesis of mesoporous carbon，through the quality changes of the pro- portion of carbon source，carbon source and carbon chain length of the template and the template types and to explore its effect on mesoporous carbon materials in the synthesis process，the particle size and par- ticle size range．The results show that when the phenolic resin thermal polymerization time １．０ h，meso- porous carbon pore size was uniform，dense pore structure；when the template agent and phenolic resin in the mass ratio of １．０∶１．０ ，mesoporous carbon pore formation developed，specific surface area and large pore volume；in determining the carbon source polymerization time was １．０ h．The template and phenolic resin mass ratio is １．０∶１．０ ，compared with template P１２３ and F１２７ two kinds of template，results show