气相色谱法测定氢化油脂加工食品中反式脂肪酸含量.pdf

6 1 Vol. 6 No. 1 2015 1 Journal of Food Safety and Quality Jan. , 2015 * 高 宏 , 徐 慧, 贾 涛, 郭芳芳 (, 210042) 摘 要: 目的 方法 HP-88 (30 m×0.25 mm×0.20 μm)43 , 结果 30 m , 3~100 µg/mL TFA (R 0.9990), (RSD 6%), 85.3%~91.8%, 0.01 g/100 g; 100 m 1 ; , (t-C16:1)(t-C18:1) 结论 , 关键词: ; ; ; Determination of the trans-fatty acids in hydrogenated fat processed foods by gas chromatography * GAO Hong , XU Hui, JIA Tao, GUO Fang-Fang (Jiangsu Test Center for Physics and Chemistry , Nanjing 210042, China) ABSTRACT: Objective To develop a method for the determination of trans-fatty acids in processed food by hydrogenated oil using gas chromatography(GC). Methods 43 kinds of fatty acids were separated qualitatively and quantitatively by HP-88 qualified column(30 m×0.25 mm×0.20 μm), and the method was used to detect trans-fatty acid concentration of biscuits, cakes, ice cream, milk tea, coffee and other processed foods. Results The trans-and cis-fatty acids were separated. It had a good linearity at concentrations of 3~100 µg/mL, the RSD was within 6.0%, the recover