X荧光分析-公开课件.pptVIP

第三部分 X荧光成分分析 1 方法特点 2 分析原理 3 仪器构成 4 WDS-XRF 5 EDS-XRF 6 定量分析 1 方法特点（1） 1 方法特点（2） 1 方法特点 (3) 1 方法特点（4） 1 方法特点（5） 1 方法特点（6） 2 分析原理（1） 2 分析原理（2） 2 分析原理（3） 2 分析原理（4） 3 仪器构成（1） 3 仪器构成（2） 4 WDS-XRF(1) 4 WDS-XRF(2) 4 WDS-XRF(3) 4 WDS-XRF(4) 4 WDS-XRF(5) 4 WDS-XRF(6) 4 WDS-XRF(7) 4 WDS-XRF(8) 4 WDS-XRF(9) 4 WDS-XRF(10) 5 EDS-XRF (1) 5 EDS-XRF (2) 5 EDS-XRF (3) 5 EDS-XRF (4) 5 EDS-XRF (5) 5 EDS-XRF (6) 5 EDS-XRF (7) 5 EDS-XRF (8) 5 EDS-XRF (9) 6 定量分析（1） 6 定量分析（2） 6 定量分析（4） 第二部分. X荧光成分分析 第二部分. X荧光成分分析 The high resolution lithium drifted silicon X-ray detectors provide low detection limits, few spectral interferences, and accuracy over a wide range of concentrations. These detectors are able to separate the electron energy coming from the sample into elemental components, which in turn are translated into ratio, qualitative, or quantitative elemental data in spreadsheet or word processor formats. Additionally, the tube voltages on EDSXRF are quite low and the entire instrument is plugged into a standard wall socket. WDSXRF requires filtered voltage at 220 V. 第二部分. X荧光成分分析 Advantages: (1) NON-DESTRUCTIVEIn the vast majority of cases, analyzed samples are not destroyed or changed by exposure to x-rays. They can thus be saved for future reference or used for other types of testing that may be destructive. (2) MINIMAL PREPARATION Many samples can be examined with little or no pre-treatment. Many of the alternative techniques require dissolution procedures that are both time-consuming and costly in terms of the acids or other reagents required. 第二部分. X荧光成分分析 Advantages: (3) FASTX-ray spectrometry enables chemical compositions to be determined in seconds. (4) EASY TO USEModern instruments run under computer control, with effective software to handle measurement set-up and results calculation. Tasks that once required the constant attention of a trained analyst can now be handled by skilled operators — or even carried out by fully automated systems. 第二部分. X