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层状纳米羟基磷灰石的结晶性能及形成机理-IngentaConnect.pdf

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40 5 715 40 5 Vol. 40No. 5 2 0 1 2 5 JOURNAL OF THE CHINESE CERAMIC SOCIETY M a y 2 0 1 2 1,2 2 1,2 2 1,2 1,2 (1. 2. 510640) (nano-hydroxyapatiten-HA)X Fourier 24 h HA n-HACaHPO 2.0 4 TQ172 A 0454–5648(2012)05–0715–08 2012–04–23 10:40:35 /kcms/detail/11.2310.TQ1040.014.html Crystal Properties and Formation Mechanism of Layered Nano-Crystalline of Hydroxyapatite ZHENG Zhiwen1,2 2 1,2 2 1,2 1,2 LIU Xiaojian ZHAO Naru ZHANG Shuhua WEI Kun WANG Yingjun (1. National Engineering Research Center for Human Tissue Restoration Reconstruction; 2. School of Materials Science and Engineering, South China University of Technology, Guangzhou 510640, China) Abstract: The nano-crystalline of hydroxyapatite (n-HA) with an ordered multi-layered structure was synthesized with a mono alkyl phosphate as a template. The effect of the condition on the microstructure and morphology was investigated via transmission electron microscopy, X-ray diffraction and Fourier transform infrared spectroscopy, respectively. The formation mechanism of the n-HA with layered structure was proposed according to the experimental results. The results showed that the nano-crystalline with the uniform structure can be formed after 24 h. The synthesized products were mainly n-HA under alkaline condition, and the products were mainly CaHPO4 under acidic condition. The shape and size of nano-crystals were relatively homogeneous at a mass ratio of alcohol to water of 2