Ｘ射线衍射分析　XRD专业教程.pptVIP

Brief tutorial on X ray powder diffraction data analysis Some bibliography X-ray powder diffraction (XRPD): brief summary Qualitative Analysis: evaluate your pattern and look for possible phase(s) Quantitative Analysis: Rietveld refinement X-ray Powder Diffraction NOTE (multi-) peak fitting routines 1 To Select diffraction peaks 1) position the mouse at the peak maximum and 2) pres the p key Check box to refine or fix the parameters * Dr Carlo Meneghini Dip. Di Fisica, Università di Roma Tre meneghini@fis.uniroma3.it II African School on X-ray in materials 19-24 Jan. 2009 http://webusers.fis.uniroma3.it/~meneghini/software.html XRPD_tutorial.exe Pwder diffraction: technique and data analysis B.E. Warren, X-Ray Diffraction (Addison-Wesley, 1990). H.P. Klug and L.E. Alexander, X-Ray Diffraction Procedures (Wiley Interscience, 1974). B.D. Cullity, Elements of X-Ray Diffraction (Wiley, 1978). Modern Powder Diffraction Reviews in Mineralogy, Volume 20 D.L. Bish and J.E. Post, Editors Mineralogical Society of America, 1989. Fundamentals of Crystallography IUCr Texts on Crystallography -2 C. Giacovazzo, Editor Oxford Science Publication, 1992. The Rietveld Method IUCr Monographs on Crystallography - 5 R.A. Young, Editor Oxford Science Publication, 1993. X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials H.P Klug and L.E. Alexander Wiley-Interscience, 1974, 2nd edition. Defects and Microstructure Analysis by Diffraction R.L. Snyder, J. Fiala and H.J. Bunge, IUCr Monographs on Crystallography, Vol 10, Oxford Science Publications, 1999. Bibliography On line resources /xrd/resources.htm http://www.ccp14.ac.uk/ / International centre for diffraction data The collaborative computational projects A resource page for XRD Atomic distribution in the unit cell Peak relative intensities Unit cell Symmetry and size Peak positions a c b Peak shapes Particle size and defects Background Diffuse scattering, sample holder, matrix, amorphous phas