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选择性保护的1，4，7-三氮环壬烷的合成与应用
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目录
摘要······························································································································2
英文摘要······················································································································2
前言······························································································································3
第一章 文献综述
1.1前人工作·······································································································4
1.2 TACN衍生物的合成······················································································5
1.3 实际应用······································································································7
1.4本文研究目的·······························································································8
1.5 本课题研究的前景·····················································································11
1.6 小结·············································································································11
第二章 实验部分
2.1仪器及药品··································································································12
2.2 实验步骤·····································································································12
2.2.1 1，4，7-三对甲苯磺酰基-1，4，7三氮环壬烷的制备············
2.2.2 HBr/CH3COOH溶液的制备·······························································13
2.2.3 选择性保护的1，4，7-三氮环壬烷的合成································14
2.2.4 氯甲基苯并咪唑(CBZ)的制备·······················································14
2.2.5 带保护基的配体的合成·································································14
2.2.6 去保护的配体的合成·····································································14
第三章 实验结果及讨论···························································································15
3.1 制备1，4，7-三对甲苯磺酰基-1，4，7三氮环壬烷的影响因素·······15
3.2 制备HBr/CH3COOH溶液时的影响因素······································
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