材料现代分析测试方式射线衍射.ppt

* Let’s first refresh our memory on Bragg Brentano geometry. In this geometry the sample surface bisects the scattering angle. Because the scattering angle is the same irrespective the part of the beam, the diffracted beam is focused. The positon of this focus point is at exactly the distance from the sample surface as the tube focus. At that position we had placed a narrow slit to obtain the optimal resolution (Receiving slit). 从线形增宽中获得晶粒尺寸及微观应力的信息，必须完成两项工作： 1）从B中扣除b，求β。 2）从β中再分离出m和n。 第一项工作可用式(B)完成，但需知道f(x)，而f(x)难以知晓。 当然可以根据式(A)，用实验得到的h(x)、g(x)线形数据，通过