ICPMS日常保养和维护技术应用.pptVIP

* X Series ICP-MS The key design features are: - Worlds smallest bench-top ICP-MS Highest throughput with protocol compliance Tailored configurations Maintenance free mass spectrometer Proven PlasmaLab? Windows? software Responsive CarePlan? Support Package Plug-and-Play Upgradability * Xi Interface - Performance Specifications Sensitivity, Background and Stability of the Basic instrument fitted with the Xi interface Data in cps using a 1ppb mixed element standard Data taken from the standard Pre Delivery Short Term Stability Test * This system was proven to be matrix tolerant, with a long-term drift of typically 10% when running high matrix samples such as borehole tap waters for 4.5 hours. The reduction in polyatomic species and reduced background levels afforded by the new interface gave good detection limits for elements that typically suffer from interferences in heavy matrices (i.e. borehole tap waters). LOD for Fe was 3.4ppb well within the 1/10th PCV criteria of 20ppb Background levels at mass 5 and 220 were 0.05cps a factor of 10x improvement to the std system Although the response was 10x less than the std system, the signal to noise ratio remained the same, also up to 500ppm measurements could be obtained in the same run as sub ppb levels This work shows that it is possible to determine 21 elements to DWI and NS-30 analytical requirements plus an additional 5 elements using a single analytical technique. As well as easily meeting the required detection limits for the trace elements such as Pb, the LOD for Pb of 0.088 ug/L will easily fulfil future legislation of 1ppb LOD. * Maintenance Free Mass Spectrometer ? The quadrupole is now housed in a minimum volume chamber for faster pump down but there has been no compromise on the size of the quadrupole rod set in order to reduce the size of the spectrometer. The quad. still has 230mm x 12mm diameter rods with pre-filters this gives The large quad rods and excellent vacuum provide abundance sensit