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Accessed from 128.83.63.20 by nEwp0rt1 on Tue Nov 29 23:32:55 EST 2011
NF 30 Official Monographs / Polyoxyl 1917
C: To a solution (1 in 20) add bromine TS, dropwise: the Congealing temperature 〈651〉: between 37° and 47°.
bromine is decolorized. Acid value 〈401〉: not more than 2.
Specific gravity 〈841〉: between 1.05 and 1.06. Hydroxyl value 〈401〉: between 25 and 40.
Viscosity 〈911〉: between 600 and 850 centipoises at 25°, a Saponification value 〈401〉: between 25 and 35.
capillary viscometer being used. Water, Method I 〈921〉: not more than 3.0%.
Acid value 〈401〉: not more than 2.0. Heavy metals, Method II 〈231〉: 0.001%.
Hydroxyl value 〈401〉: between 65 and 80. Free polyethylene glycols—Transfer about 6 g, accurately
Iodine value 〈401〉: between 25 and 35. weighed, to a 500-mL separator containing 50 mL of ethyl ace-
Saponification value 〈401〉: between 60 and 75. tate. Dissolve completely, then add 50 mL of sodium chloride
Water, Method I 〈921〉: not more than 3.0%. solution (29 in 100), shake vigorously for 2 minutes, and allow
Residue on ignition 〈281〉: not more than 0.3%. to separate for 15 minutes. If separation is incomplete, carefully
insert the separator into the well of a steam bath for short time
Heavy metals, Method II 〈231〉: 0.001%. intervals. Repeat this technique as many time
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