Nexus 470 FTIR 红外光谱仪学习手册.pdf

Thermo-Nicolet Nexus 470 FTIR User’s Guide Version 2.1 Edited by Dr. Hartmut G. Hedderich 7/15/2013 The following guide describes the use of the Thermo-Nicolet Nexus 470FTIR spectrometer. The guide is intended to assist instrument users after the initial training session. Thermo-Nicolet Nexus 470– User’s Guide, Ver. 2.1 Thermo-Nicolet Nexus 470 FTIR – User’s Guide, Ver.2.1 edited by Dr. Hartmut G. Hedderich 1. Hardware: The Nexus FTIR is a compact bench unit. It contains separate compartments for light source, sample, beamsplitter and detector. The Nexus 470 FTIR is ALWAYS(!) turned on. Never try to turn the system off! The detector is liquid nitrogen cooled. It needs to be filled prior to the experiment – cool- down time is in the order of 10-15 minutes. The system needs to be purged with nitrogen in order to suppress water and carbon dioxide bands. There is a valve marked FTIR on the manifold which will supply nitrogen gas from the liquid nitrogen tank boil-off. Do not forget to turn the valve off when you are done with your experiment! Hardware configuration and data collection is fully computer-controlled via OMNIC software (Version 6.2). In the standard configuration the NEXUS is running with the Smart-iTR module. For gas samples and certain liquid samples the system can be re-configured to a standard FTIR with cell holder. 1 Thermo-Nicolet Nexus 470– User’s Guide, Ver. 2.1 2. Samples The Nexus FTIR can measure gaseous, liquid and solid samples. The standard configuration uses the Smart-iTR setup. The Smart