7.3万吨年粗苯加氢精制工艺设计.docxVIP

附 录 MACROBUTTON MTEditEquationSection2 SEQ MTEqn \r \h SEQ MTSec \r 1 \h SEQ MTChap \r 1 \h 摘 要 本次设计的主要任务是处理量为7.3万吨/年的粗苯加氢精制工艺的设计，因而采用了能够持续性对筛板塔进行精馏的基于低温加氢溶剂萃取原理的化工装置。 通过分离轻重组分于两苯塔中，回收的重质苯于塔釜中的操作后，利用加氢反应对轻苯原料进行硫化氢，氨气等的脱去，并且将过程产物继续通入预精馏塔、萃取精馏塔 纯苯塔和二甲苯塔之中，经过以上操作，对粗苯原料进行了多步纯化，获得了合格的纯净苯以及纯净甲苯等产品。 在本次设计中，为了得到设计所需要的参数，在设计过程中为了达到设计的要求，在设计过程中，在进行了衡算物料、衡算热量、计算塔的具体工艺尺寸、计算全部塔板的负荷性能高低，计算各类其它设备的操作之后，获得了本次设计中所需要全部参数，其中进料量，塔顶液体流量，塔底釜液流量，塔径，塔高，板间距，精馏段实际塔板数，提馏段塔板数等参数分别为109.5Kmol/h,92.682Kmol/h,16.639Kmol/h，1.6m,24.45m,0.46m，17块，17块，并且对人孔数的数量设置为7个，对板间距于人孔间的数值大小为0.7m,板间距于进料处的数值大小为1m。 关键词 加氢精制；连续精馏筛板塔；两苯塔；苯；甲苯 Abstract The main task of this design is to design the crude benzene hydrofining process with a processing capacity of 73,000 tons/year. The process flow of solvent extraction and low-temperature hydrofining is adopted. For this reason, the chemical equipment of continuous distillation sieve plate column is selected. By?separating?the?light?and?heavy?components?in?the?two?benzene?towers,?the?recovered?heavy?benzene?is?operated?in?the?tower?kettle,?and?the?hydrogenation?reaction?is?used?to?remove?the?hydrogen?sulfide?and?ammonia?gas?from?the?light?benzene?raw?materials,?and?the?process?products?are?continuously?passed?into?Among?the?pre-rectification?tower,?extractive?distillation?tower?pure?benzene?tower?and?xylene?tower,?after?the?above?operations,?the?crude?benzene?raw?material?was?purified?in?multiple?steps?to?obtain?qualified?pure?benzene?and?pure?toluene?and?other?products.In?this?design,?in?order?to?obtain?the?parameters?required?by?the?design,?in?order?to?meet?the?design?requirements?in?the?design?process,?during?the?design?process,?the?materials,?heat,?the?specific?process?size?of?the?tower?were?calculated,?and?all?the?towers?were?calculated.?The?load?performance?of?the?plate?is?calculated.?After?calculating?the?operation?of?various?other?equipment,?all?the?parameters?required?in?this?design?are?obtained,?including?the?amount?of?feed,?the?liquid?flow?at?the?top?