毕业设计—年产20万吨氯苯工艺设计（包含图纸）.docxVIP

年产20万吨氯苯精制工艺设计 学 院： 专业班级： 学生姓名： 指导教师： 成 绩： 年 月 日 摘 要 作为多种有机物的合成原料，氯苯的制备和利用在工业上已经有了很长的历史，基于氯苯制备的精制优化是尤为关键的，有必要设计出具有满足市场需求且制备过程具有可行性和可操作性的工艺流程。氯苯工艺包括氯化反应的气液反应和蒸馏、吸收等多种分离，以及多相反应器在生产平衡控制中起着关键作用。如何实现年产20万吨精制氯苯工艺流程的优化和设计，提高产物转化率以及产率和纯度是科研工作者所正在探究的方向，这也具有重要的工业前景和产业意义。本论文结合氯苯的高产量工业流程设计，具体化去探讨该流程设计，本论文中实验采用苯和氯气作为原料，实验通过改变试剂与和反应物的比例，反应体系压强值，温度，气液反应条件等等，找到以上条件对反应的影响，得出可以使得产率达95%以上的最大收率和纯度的最佳反应流程，通过对流程设计中的各环节反应条件和原理配比等进行优化，并且通过设计中加入苯的冷凝器和吸收塔，间接减少了反应器中副反应的发生，节约了原料苯的用量和消耗，增加冷却回流系统来保证产品回收和气压的均衡稳定性，回收不仅可以增加哦效益，也可以降低原料的支出消耗，结合副产物的理化性质进行结晶和蒸馏优化，可以实现高效规模回收，将其应用于化工厂大量制备来实现清晰操作简便的工业流程，达到年产20万吨氯苯精制的工艺实现。 关键词：氯苯 高产量 工业设计 反应条件 Abstract In this paper,as a raw material for the synthesis of various organic compounds, the preparation and utilization of chlorobenzene has a long history in industry. The refining optimization based on the preparation of chlorobenzene is particularly critical. It is necessary to design a process which can meet the market demand and has the feasibility and operability of the preparation process. Chlorobenzene process includes gas-liquid reaction of chlorination reaction, distillation, absorption and other separation, and multiphase reactor plays a key role in production balance control. How to optimize and design the process flow of refined Chlorobenzene with an annual output of 200000 tons, and improve the conversion rate, yield and purity of products are the research direction of scientific researchers, which also has important industrial prospects and industrial significance. This paper combined with the high-yield industrial process design of chlorobenzene, specifically to explore the process design. In this paper, benzene and chlorine were used as raw materials in the experiment. Through changing the ratio of reagent and reactant, the pressure value of reaction system, temperature, gas-liquid reaction conditions and so on, we found the influence of the above conditions on the reaction, and obtained the maximum yield and purity that