直接测汞仪测定食品中总汞含量及结果分析.docxVIP

直接测汞仪测定食品中总汞含量及结果分析 直接测汞仪测定食品中总汞含量及结果分析 Hans Journal of Food and Nutrition Science 食品与营养科学, 2021, 6(3), 181-187 Published Online August 2021 in Hans. Determination of Total Mercury in Food by Direct Mercury Analyzer Lei Feng, Chaowen Pu*, Heng Li, Renping Zhang Center for Disease Control and Prevention of Fuling District of Chongqing, Chongqing Received: Aug. 6th , 2021; accepted: Aug. 18th , 2021; published: Aug. 28th , 2021 Abstract Objective: To establish rapid determination of total mercury in solid and liquid forms of food, an elemental mercury analyzer (DMA-80) was applied in 9 kinds of food, including grains, meats, ed-ible fungus, eggs, salts, vegetables, milk and dairy products, mineral water, canned food for infants, the analytical results were compared to the commonly used national standard method atomic flu-orescence spectroscopy. Methods: Samples did not need special pretreatment and can be used by direct mercury analyzer to determine the total mercury. Results: According to the experimental conditions, the total mercury was determined by direct mercury analyzer, the sample decomposi-tion time was 2 min, the decomposition temperature of grain and other plant foods was 650?C, and the decomposition temperature of meat was 850?C. A linearity was obtained over the range of 0.0- 20.0 ng under the optimum conditions, y = ?0+ 0 ? 02, the cor-relation coefficient was greater than 0.999, recovery rate was 91.0%-102.9%, the relative stan-dard deviation of the determination results was 1.36%-2.87%, and the detection limit was 0.4 μg/kg. Conclusions: There was no statistically significant difference compared with atomic fluo-rescence spectrometry, and the method is convenient, rapid, accurate, sensitive and repeatability, it can save a large amount of reagent cost and its environmentally friendly, the method was sug-gested as a rapid method to determine total mercury for inspection of food and agricultur