荧光磁性纳米材料的制备与重金属离子的检测论文.docVIP

题目荧光磁性纳米材料的制备与重金属离子的检测 PAGE I PAGE I PAGE I PAGE I 荧光磁性纳米材料的制备与重金属离子的检测 摘 要 我们采用溶剂热法合成四氧化三铁纳米微粒，然后采用分子模板法并利用TEOS的水解反应在其四氧化三铁纳米微粒包覆二氧化硅，便得到磁性介孔微球。我们对其进行了表征和分析，用所得的SEM图像、氮气吸附脱附等温线和磁滞回线，证明了其球形的形貌、介孔的存在和超顺磁性。最后将罗丹明连接至其表面，合成了多功能磁性介孔微球。用合成的多功能磁性介孔微球来实现对重金属离子的快速检测、高效吸附。荧光分子探针通常由三部分组成 ??：识别基团（receptor）、荧光基团（fluorophore）和连接体部分（spacer）识别基团决定了探针分子的选择性和特异性，报告基团则决定了识别的灵敏度，而连接体部分则可起到分子识别枢纽的作用。 关 键 词：磁性介孔微球；重金属离子；检测；荧光分子探针 PAGE IV PAGE IV PAGE PAGE 36 Preparation and Fluorescent Detection of Heavy Metal Ions in Magnetic Nanomaterials Abstract We use solvothermal synthesis of iron oxide nanoparticles, and then using molecular template and using TEOS hydrolysis reaction in which iron oxide-coated silica nanoparticles, we get the magnetic mesoporous microspheres. We were characterized and analyzed by SEM images obtained by nitrogen adsorption-desorption isotherms and hysteresis loops, proved its spherical morphology, and the presence of superparamagnetic mesoporous. Finally, connected to the surface of the rhodamine synthesized mesoporous multifunctional magnetic microspheres. Multifunctional magnetic mesoporous synthetic microspheres to achieve rapid detection of heavy metal ions, high adsorption. Fluorescent probe is usually composed of three parts [1]: a group identification (receptor), fluorophores (fluorophore) and a connecting portion (spacer) group identification determines the selectivity and specificity of the probe molecules, the reporter group determines the recognition sensitivity, can play the role of molecular recognition part hub and connector. Key words: Magnetic Mesoporous Microspheres; Heavy Metal ions; Detection; Fluorescent Molecular Probes 目 录 TOC \o 1-3 \h \z \u 3390 1 绪论 1 27959 1.1概述 1 26606 1.2介孔材料国内外研究现状 2 21648 1.2.1国内现状 2 12873 1.2.2国外现状 2 16497 1.3课题背景 3 10606 1.3.1荧光分析原理 3 22472 1.3.2荧光素探针和磁性纳米材料的简介 5 26040 1.4硅