Agilent Applying the 5975 inert MSD to the Higher Molecular Weight Polybrominated Diphenyl Ethers (PBDEs)说明书用户手册.PDF

Applying the 5975 inert MSD to the Higher Molecular Weight Polybrominated Diphenyl Ethers (PBDEs) Application Environmental, Component Testing Author This note presents the full scan spectra obtained for the PBDEs over the extended mass range of Harry F. Prest the 5975 inert MSD. The polymeric sample prepa- Agilent Technologies, Inc. ration and extraction protocols are cited elsewhere Santa Clara, CA and supply two approaches to PBDE USA determinations [1]. Abstract Experimental A previous application note presented results for analysis PBDE standards were acquired from Cambridge of the polybrominated diphenyl ethers (PBDEs) in poly- Isotope Laboratories (Andover, MA) and mers using the 5973N inert MSD [1]. Mass spectra were AccuStandard (New Haven, CT). presented and interpreted for all of the important PBDEs. The new 5975 inert MSD provides many new features and Instrumental Configuration and Conditions improvements with expanded mass range to 1050 u being The 6890 GC configuration and conditions are but one. This note presents the full spectra of the octa-, given in the previous application note [1]. The nona and decabrominated biphenyls ethers including ions