Agilent A Total Solution for the Analysis of Melamine and Cyanuric Acid in Pet Food by GC MS and Aqueous Normal-Phase LC MS MS 说明书用户手册.PDF

A Total Solution for the Analysis of Melamine and Cyanuric Acid in Pet Food by GC/MS and Aqueous Normal-Phase LC/MS/MS Application Food Authors packages of pet food in the past year. Consequently, it became a hot issue to determine the content of Wei Luan and Yanyan Fang melamine and cyanuric acid in pet food and related Agilent Technologies (Shanghai) Co., Ltd. raw materials worldwide. 412 Ying Lun Road Shanghai 200131 A screening method using GC/MS for both these P. R. China compounds was published by the U.S. FDA [1]. According to this procedure, the detection limit for Jerry Zweigenbaum GC/MS screening method is 10 µg/g using a Agilent Technologies, Inc. trimethylsilyl (TMS) derivatization process before 2850 Centerville Road injection. Although this method is used for screen- Wilmington DE 19808 ing, it could be used as well for confirmation and USA quantitation using the SIM/SCAN function of the Agilent 5975. In comparison with the GC/MS method, the LC/MS/MS method presented here Abstract