Agilent Determination of Nitro-Polycylic Aromatic Hydrocarbons in Air Particulates using GC Triple Quadrupole MS System Application Note说明书用户手册.PDF

Determination of Nitro-Polycyclic Aromatic Hydrocarbons in Air Particulates Using the Agilent 7000A Triple Quadrupole GC/MS System Application Note Environmental Authors Abstract Frank David The analysis of nitro-polycyclic aromatic hydrocarbons (nitro-PAHs) in air particulates Research Institute for Chromatography was performed by capillary GC in combination with the Agilent 7000A Triple Pres. Kennedypark 26, B-8500 Kortrijk Quadrupole GC/MS system (G7010AA) operated in multiple reaction monitoring Belgium (MRM) mode. While classical methods for the analysis of nitro-PAHs are based on GC/MS analysis by a single quadrupole in the selected ion monitoring (SIM) mode Matthew S. Klee after labor-intensive sample preparation or on multidimensional GC/MS, direct analy- Agilent Technologies, Inc. sis of the crude air particulate extract could be performed due to the enhanced selec- 2850 Centerville Road tivity of the MS/MS detection mode. Nitro-PAHs could be detected in a real sample at Wilmington, DE 19808 low pg/µL level, corresponding to pg/m3 in air samples. USA Introduction Sampling Air particulate samples were taken using a high-volume sam- Nitro-polycyclic aromatic hydrocarbons (nitro-PAHs) are pler (Anderson Graseby, USA) on glass fiber filters, backed-up among the most toxic, carcinogenic, and mutagenic sub-