(8.5)--任务5发动机燃料实际胶质的测定.pptVIP

Task 5 determination of actual gelatin in engine fuel Ⅰ. Determination of actual gelatin in engine fuel 1．Purpose of this training. (1) Be familiar with the principle and method of determination of actual colloid of oil products (GB/T 509-1988). (2) Master the operational skills in the determination of existent gum in oil products 2. Instruments and Reagents (1) instrument oil bath (Figure 8-11); No mouth high glass beaker (1, 100mL); Measuring cylinder (1, 25mL); Straws (1, 25mL); Flowmeter (1); Air filter (one containing cotton and glass beads); Thermometer (1, 0~360 ℃); Blower, air compressor or air supply main; Electric heating plate; Chrome-plated crucible tongs; Mineral oil (open flash point not less than 310 ℃). (2) reagent benzene (chemically pure); Acetone (chemically pure), ethanol-benzene mixture [prepared by 1: 1 volume ratio of 95% ethanol (chemically pure) and benzene (chemically pure) ] ; sodium sulfate (chemically pure); Jet fuel. 3. Method OverviewThe 25mL sample is evaporated under the specified conditions of instrument, temperature and air flow, and then the resulting residue is weighed and expressed as the actual gum mass (mg/100mL) contained in the 100mL sample. 4. Preparation: (1) treatment of obvious water marks in the sample when the sample clearly contains water marks, a proper amount of newly calcined sodium sulfate should be added into the sample first, and after shaking for 10~15min, filter the sample with filter paper. (2) The oil bath is filled with oil and an appropriate amount of mineral oil is injected into the oil bath. It is required that the oil bath can be filled when it is heated to the test temperature after the bath cover is covered. (3) Install the thermometer and insert the thermometer into the orifice of the bath cover with a cork to make the mercury ball 40~50mm away from the cover surface. When needed, insert the contact thermometer into another orifice on the bath cover. When me