甲基异丁基甲酮原子吸收法测定金的准确度研究.docxVIP

甲基异丁基甲酮原子吸收法测定金的准确度研究 摘要：本研究旨在研究甲基异丁基甲酮原子吸收法测定金的准确度以及影响参数。实验中，采用甲基异丁基甲酮原子吸收光谱法，考察金与甲基异丁基甲酮（MBT）相关性。实验参数包括MBT质量，溶剂质量，温度，示波器设置，以及比色皿类型的等因素，比较其精度的差异。实验结果表明，与基线情况相比，当MBT的质量为30 g之后，峰高显著降低，影响了测定精度；在溶剂的质量为3.0 mL的情况下，温度的升高导致金的激发峰更早出现；在示波器设置为5 V 情况下，频率的上升会影响测定精度；比色皿采用16 廓度试管比较精准。综上所述，本实验可有效检测甲基异丁基甲酮原子吸收法测定金的准确度，并有利于进一步提高测定金水平的精度。 Abstract：This study aimed to investigate the accuracy of gold determination by methyl isobutyl ketone atomic absorption spectrometry and the influencing parameters. In the experiment, the methyl isobutyl ketone (MBT) atomic absorption spectrometry was used to investigate the correlation between gold and MBT. The experimental parameters included the mass of MBT, the mass of solvent, the temperature, the oscilloscope setting, and the type of colorimetry were compared for the accuracy difference. The experimental results showed that, compared with the baseline, the peak height was significantly decreased after the mass of MBT was 30 g, which affected the determination accuracy; the temperature increased in the case of the mass of solvent was 3.0 mL, and the gold excitation peak appeared earlier; the frequency rise in the case of the oscilloscope was set to 5 V would affect the determination accuracy; the 16 steps tube colorimetry was more accurate. In summary, this experiment can effectively detect the accuracy of gold determination by methyl isobutyl ketone atomic absorption spectrometry and beneficial to further improve the accuracy of gold determination. Keywords：Methyl isobutyl ketone; Atomic absorption; Gold; Accuracy