以TiOSO4为原料水热合成纳米TiO2及其光催化性能研究的中期报告.docxVIP

以TiOSO4为原料水热合成纳米TiO2及其光催化性能研究的中期报告 摘要： 本研究以TiOSO4为原料，通过水热合成法制备了纳米TiO2，并对其光催化性能进行了研究。采用X射线粉末衍射（XRD）、透射电镜（TEM）和紫外-可见漫反射光谱（UV-vis DRS）等技术对样品进行了表征。结果表明，在水热反应温度为180℃，反应时间为24 h的条件下，制备得到的纳米TiO2晶体结构完整、粒径大小均匀，平均粒径为16 nm。纳米TiO2的紫外吸收较强，表明样品具有良好的光催化性能。通过光催化降解甲基橙的实验，发现TiO2的光催化性能较好，在紫外光照射下，甲基橙的降解率可达85%。 关键词：水热合成；纳米TiO2；光催化性能；甲基橙 Abstract: In this study, nano TiO2 was synthesized via a hydrothermal method using TiOSO4 as the raw material, and its photocatalytic performance was investigated. The samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and UV-Visible diffuse reflectance spectroscopy (UV-vis DRS). The results showed that the nano TiO2 crystals obtained under the conditions of a hydrothermal reaction temperature of 180°C and reaction time of 24 h had a complete crystal structure and uniform particle size, with an average particle size of 16 nm. The nano TiO2 had strong UV absorption, indicating good photocatalytic performance. The photocatalytic degradation of methyl orange was conducted, and it was found that the TiO2 had good photocatalytic performance, with a degradation rate of methyl orange of up to 85% under UV irradiation. Keywords: hydrothermal synthesis; nano TiO2; photocatalytic performance; methyl orange