过渡金属氟化物和氧化物纳-微米晶的制备、表征及其性质的中期报告.docxVIP

过渡金属氟化物和氧化物纳-微米晶的制备、表征及其性质的中期报告 【摘要】 本中期报告主要介绍了过渡金属氟化物和氧化物纳-微米晶的制备、表征及其性质研究的进展情况。制备过程采用了水热法、溶胶-凝胶法、物理气相沉积法等方法。通过X射线衍射、扫描电子显微镜、透射电子显微镜等方法对所得样品进行了表征。结果表明，所制备的过渡金属氟化物和氧化物纳-微米晶具有优异的晶体结构、单分散性、高比表面积和活性，可以广泛应用于电化学传感器、光电催化等领域。 【关键词】过渡金属氟化物；氧化物纳-微米晶；制备；表征；性质 【Abstract】 This midterm report mainly introduces the progress of the preparation, characterization and properties of transition metal fluorides and oxide nano-microcrystals. Preparation processes using hydrothermal method, sol-gel method, physical vapor deposition method and other methods. The obtained samples were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and other methods. The results show that the prepared transition metal fluoride and oxide nano-microcrystals have excellent crystal structure, monodispersity, high surface area and activity, and can be widely used in electrochemical sensors, photoelectrocatalysis and other fields. 【Keywords】transition metal fluoride; oxide nano-microcrystals; preparation; characterization; properties