ASTM D5932-08(2013)e1 美国材料与试验协会标准.pdfVIP

Designation:D5932−08(Reapproved2013)´1

StandardTestMethodfor

Determinationof2,4-TolueneDiisocyanate(2,4-TDI)and2,6-

TolueneDiisocyanate(2,6-TDI)inAir(with9-(N-

Methylaminomethyl)AnthraceneMethod)(MAMA)inthe

Workplace1

ThisstandardisissuedunderthefixeddesignationD5932;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.

ε1NOTE—Editorialcorrectionsweremadeto8.14.8and11.2.1inMarch2015.

1.Scopesolution,whichcorrespondstoconcentrationsof0.002to

1.1Thistestmethodcoversthedeterminationofgaseous0.077mg/m3ofTDIbasedona15-Lairsample.This

2,4-toluenediisocyanate(2,4-TDI)and2,6-toluenediisocya-correspondsto0.28to11ppb(V)andbracketstheestablished

nate(2,6-TDI)inairsamplescollectedfromworkplaceandTLVvalueof5ppb(v).

ambientatmospheres.1.6Afieldblanksamplingsystemisusedtocheckthe

1.2Differentialairsamplingisperformedwithasegregat-possibilityofcontaminationduringtheentiresamplingand

ingdevice.2,3Thegaseousfractioniscollectedonaglassfiberanalysis.

filter(GFF)impregnatedwith9-(N-methylaminomethyl)an-1.7ThevaluesstatedinSIunitsaret