固相微萃取-气相色谱-质谱法测定水体中半挥发性有机污染物.pdfVIP

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固相微萃取-气相色谱-质谱法测定水体中半挥发性有机污染物.pdf

固相微萃取-气相色谱-质谱法测定水体中半挥发性有机污染物

吕天峰;张宝;滕恩江;吕怡兵

【摘要】GC-MSwithsolidphasemicro-extraction(SPME)wasappliedto

thedeterminationof24semivolatileorganiccontaminants(SVOCs)in

water.ToattainahigherefficiencyinSPME,85μmpolyacrylatefibrewas

selectedascoatingforthemicro-extractor,andtheextractionwascarried

outat50℃for30min.TheanalytewereseparatedonDB-5MScapillary

columnanddetectedbyEIionsourcewithwholescanningmonitoring

mode.Linearrelationshipsbetweenvaluesofpeakareaandmass

concentrationofthe24SVOCswerekeptinthesamerangeof

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