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ph计使用说明书.doc

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1.Whenunpacking,checkelectrodeforpossiblemechanicaldamagetothemembrane(1),thediaphragm(3)orthebody(2).electrodessubjecttocomplaintsmustbereturnedtousortoouragentintheoriginalboxindicatingtheinvoicenumber.

2.takeoffwateringcap(7)andflushelectrodewithdistilledwater.

Afterrinsingwithdist.water,wipetheelectrodewithatissue.Donotrubasanincreaseoftheresponsetimemightresult.

3.removerubbercapwhichcoverstheelectrolytefillingaperture(4)orcutoffnipple(T)toensurepressureequalizationwiththeatmosphere.

4.eliminateanyairbubblesinsidethemembranespace(6)ofthemeasuringelectrodebysmoothlyswingingtheunitintheverticalplane.

5.torenewadriedoutglassmembrane,soakitforseveralhoursintheappropriatestoragesolution.itisrecommendedtostoreglasselectrodesindist.water,combinedandreferenceelectrodesinthereferenceelectrolytesolution(asunder8)

6.afteralonganddrystorageperiod,theglassmembranecanbereactivatedwithhydrofluoricacid(codeno.51-340073):theelectrodemembraneisdippedfor1min.inthissolutionfollowedbyrinsengwithdist.waterandsoakingfor12hoursinthestoragesolution.

7.electrodeswithgroundsleevediaphragm:slightlyliftthegroundsleevesothatsomereferenceelectrolytedropsout.

8.checklevelofelectrolyte(5)whichshouldbeapprox.10mmbelowrefillingaperture(4).refill,ifnecessarywith:

-3MKCl+AgCl(orderno.51340235)forelectrodeswithAg/AgClwire

-3MKCl(orderno.51340235)forhightemperatureelectrodeswithARGENTHALcartridge.

9.electrodeswithgellifiedelectrolytewithoutrefillingportaretreatedasper1,2,4,5,6,above.forstoragewerecommendasolution3mol/LKCl.

10.beforecalibratingortakingmeasurements,attentionshouldbepaidtotheinstructionsoftherelativePHinstrumentmanufacturer.Additionally,pleaserefertotheMETTLERTOLEDObrochure“practiceandTheoryofPhmeasurement

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