内容专着calcium lactate2457-乳酸钙.pdfVIP

USP35OfficialMonographs/Calcium2457

B:Mix1gwith20mLofwater,andaddsufficient6NB:Whenheated,itbecomesturbid,owingtotheseparation

aceticacidtoeffectsolution:theresultingsolutionrespondstoofcalciumhydroxide.

thetestsforCalcium〈191〉.C:ItrespondstothetestsforCalcium〈191〉.

Limitofacid-insolublesubstances—Dissolve2.0gin30Alkaliesandtheircarbonates—Aportionofit,saturated

mLof4Nhydrochloricacid,andheattoboiling.Filterthewithcarbondioxideandsubsequentlyboiled,isneutralin

mixture,washtheresiduewithhotwater,andignite:thereaction.

weightoftheresiduedoesnotexceed10mg(0.5%).Assay—Pipet100mLofTopicalSolutionintoasuitablecon-

Carbonate—Mix2gwith50mLofwater:theadditionofantainer,add50mLofwater,15mLof1Nsodiumhydroxide,

excessof3Nhydrochloricacidtothemixturedoesnotcauseand300mgofhydroxynaphtholblue,andtitratewith0.05M

morethanaslighteffervescence.edetatedisodiumVStoablueendpoint.EachmLof0.05M

Heavymetals〈231〉—Dissolve2.0gin20mLof3Nhydro-edetatedisodiumisequivalentto3.705mgofcalciumhydrox-

chloricacid,andevaporateonasteambathtodryness.Dis-ide[Ca(OH)2].

solvetheresiduein20mLofwater,andfilter.Dilutethefiltrate

withwaterto40mL,andto20mLoftheresultingsolution

add1mLof0.1Nhydrochloricacid,thenaddwatertomake

25mL:thelimitis20µ