MAO_PLA_ZnO复合涂层增强AZ31镁合金耐腐蚀性和抗菌性研究.pdfVIP

《热加工工艺》2023年月第52卷第2期

MAO/PLA/ZnO虽AZ31镁合金

复合涂层增强

耐腐蚀性和抗菌性研究

闫宏光，王欣，刘小萍

（太原理工大学新型碳材料研究院生物材料表面与界面实验室，山西太原030024)

摘要：结合微弧氧化（MAO）和浸渍涂布，在AZ31镁合金表面制备了MAO/PLA/ZnO复合涂层。运用X射线衍

射仪（XRD）、傅里叶变换红外光谱仪（FTIR）和扫描电镜（SEM)对复合涂层结构和形貌进行表征，测试了复合涂在模拟

体液(SBF)中的耐腐蚀性，研究了该涂层的抗菌性能。结果表明：由聚乳酸(PLA)和氧化锌(ZnO)纳米颗粒组成的有机-

无机涂层改善了MAO膜表面结构；复合涂层有效提升了镁合金的耐腐蚀性，腐蚀电流密度相比基底至少降低了104

倍，同时ZnO纳米颗粒的添加使得复合涂层对金黄色葡萄球菌表现出良好的抗菌性。

关键词：AZ31;MAO；复合涂层；耐腐蚀性；抗菌性

D0I:10.14158/ki.1001-3814

中图分类号：TG174.4;TG146.22文献标识码：A文章编号：1001-3814(2023)02-0097-05

StudyonCorrosionResistanceandAntibacterialPropertiesofMAO/PLA/ZnO

CompositeReinforcedAZ31MagnesiumAlloy

eCoating

YANHongguang,WANGXin,LIUXiaoping

(BiomaterialsSurfaceandInterfaceLaboratory,InstituteofNewCarbonMaterials,TaiyuanUniversityofTechnology,

Taiyuan030024,China)

Abstract:Combinedwithmicro-arcoxidation(MAO)anddipcoating,MAO/PLA/ZnOcompositecoatingwas

successfullypreparedonthesurfaceofAz31magnesiumalloy.Thestructureandmorphologyofthecompositecoatingwere

characterizedbyX-raydiffraction(XRD),Fouriertransforminfraredspectrometer(FTIR)andscanningelectronmicroscope

(SEM).Thecorrosionresistanceofthecompositecoatinginsimulatedbodyfluid(SBF)wastested,andtheantibacterial

propertiesofthecoatingwerestudied.Theresultsshowthattheorganic-inorganiccoatingcomposedofpolylacticacid(PLA)

andzincoxide(ZnO)nanoparticlesimprovesthesurfacestructureoftheMAOfilm.Thecompositecoatingeffectively

improvesthecorrosionresistanceofthemagnesiumalloy,andthecorrosioncurrentdensityisatlea