不同碱对产率影响及还原胺化方法研究.pptxVIP

工作汇报崔得运2017-2-27

试验编号碱产率cdy-399NaOH69%cdy-400KOH56%cdy-401Na2CO365%cdy-402K2CO358%cdy-403NaHCO353%cdy-404Na3PO412H2O74%cdy-405NaHPO451%cdy-406Et3N57%cdy-407DIPEA71%

试验编号R1基R2基产率备注cdy-396CH3(CH2)7H30%方法1cdy-398CH3(CH2)7P-CH3(C6H5)CH229%方法1cdy-408CH3(CH2)7CH2(C6H5)63%方法2cdy-409CH3(CH2)7CH3(CH2)750%方法2方法1：还原胺化方法2：卤代

试验编号R1基R2基备注cdy-411CH3(CH2)7Hcdy-412CH3(CH2)7CH2(C6H5)H谱不正确cdy-413CH3(CH2)7CH3(CH2)7