塑性预变形对316L奥氏体不锈钢氢脆的影响.docVIP

塑性预变形对316L奥氏体不锈钢氢脆的影响 董伟南，王艳飞，巩建鸣 南京工业大学 机械与动力工程学院 21 南京 摘要：通过对不同塑性预变形的316L奥氏体不锈钢板试样电化学充氢后进行拉伸试验，研究了塑性预变形对316L不锈钢氢脆的影响。结果表明充氢后316L。 关键词：316L奥氏体不锈钢预变形氢脆塑性损减Effect of Plastic Pre-deformation on Hydrogen Embrittlement of 316L Austenitic Stainless Steel DONG Wei-nan, WANG Yan-fei , GONG Jian-ming （College of Mechanical and Power Engineering, Nanjing University of Technology , Nanjing 21, China） Abstract：The effect of pre-deformation percentage on the hydrogen embrittlement of 316L austenitic stainless steel plate specimens was investigated by hydrogen pre-charging and tensile tests. Specimens were firstly strained to 6%, 10%, 15% and 20% of plastic strains and then hydrogen charged. After charging, the specimens were tensile to facture. The results showed that, with the increase of plastic pre-deformation percentage, the yield strength and tensile strength of 316L increased, but plasticity decreased. The strength of 316L was less affected by hydrogen charging, but the plasticity was further decreased, indicating that hydrogen embrittlement occurred. Hydrogen embrittlement susceptibility of 316L was highly dependent on the amount of plastic deformation, and the plasticity loss increased with the plastic pre-deformation increasing. Key Words: 316L austenitic?stainless steel; Pre-deformation; Hydrogen embrittlement; Plasticity loss 0 引 言 奥氏体不锈钢具有对奥氏体结构其强度采用应变强化技术制造奥氏体不锈钢高压氢储罐及其管道研究者关注的点之一。因此，通过电化学充氢及拉伸试验，研究了不同预塑性变形程度对316L奥氏体不锈钢的氢脆敏感性的影响。 1 试样制备与试验方法 试验用材料为10mm厚的商用热轧316L奥氏体不锈钢钢板，最终热处理为1080固溶处理，化学成分（质量分数）为0.17C，0.34Si，1.Mn，0.03P，0.002S，6.78Cr，10.2Ni，2.Mo，0.Cu，0.0N。沿着钢板轧制方向线切割出个，采用金相砂纸对试样标距部分进行逐级打磨直至1200#，用丙酮乙醇混合液清洗试样，用去离子水冲洗并吹干。将个在Instron5869拉伸试验机上拉伸速 mm·min-1），塑性预变形量6%、10%、15%20%。 图 常温拉伸试样尺寸Fig.1 Dimension of the tensile specimens at room temperature (mm) 每组中取一个试样进行电化学充氢电化学充氢采用0.5 mol/L的硫酸溶液，并加入为10 m/L的作为毒化剂，由于不溶于硫酸，需先将其溶于3倍体积的无水乙醇中，再加入到硫酸溶液中。充氢时试样接电源阴极，铂电极接阳极，电流密度为50 mA/cm2，充氢时间为96 h。充氢结束后，将试样迅速取出并拉伸。充氢Instron5869拉伸试验机拉伸直至断裂，拉伸速0.5mm·min-1（对应的应变速率为2.7×10-4 s-1），获得不同预量下未充氢