ccd 短波近红外光谱仪测定牛奶成分的可用性研究.pdfVIP

CCD 短波近红外光谱仪测定牛奶成分的可行性研究 1 2 1 1 1* 皮付伟 王燕岭 鲁超 王加华 韩东海 1 2 （中国农业大学食品科学与营养工程学院 北京 100083 北京英贤仪器有限公司 北京 100070 ） E-mail: caundt@cau.edu.cn 摘 要 研究了电荷耦合器件（CCD ）近红外光谱仪（NIRS ）在短波区域（700~1100nm），测定牛奶中蛋白质、脂肪、 乳糖等三种常规成分的含量。采用散射校正（MSC ）和偏最小二乘回归（PLS ）相结合的方法建立了定量模型。将短波NIRS 对未知样品的预测结果与FOSSOMATIC 4000 在的测量结果进行比较，对预测的准确性进行了考察。 关键词 近红外光谱；电荷耦合器件；偏最小二乘回归； 牛奶 中图分类号 O657.3 Analysis and Study in Components of Milk by CCD Near Infrared Spectrometer 1 2 1 1 1* Pi Fuwei , Wang Yanling , Lu Chao , Wang Jiahua , Han Donghai 1 ( College of Food science and Nutrition, China Agriculture University, Beijing, 100083 China 2Beijing INCE instrument CO., LTD., Beijing 100070, China) Abstract A charger-coupled-device-near-infrared spectrometer (CCD-NIR) was used to determine the content of protein, fat and lactose et al in milk in short wave near infrared spectral region (700~1100nm). The qualitative calibration was developed by multiple scatter correction combine with partial least square regression. The result predicted by short wave NIRS to unknown sample was compared with that by FOSSOMATIC 4000 in long wave spectral region, the accuracy was studied. Key words Near-infrared spectroscopy; charger coupled device; partial least square regression; milk 1 引 言 2 实验材料和方法 线阵电荷耦合器件（CCD ）是目前广泛应用的光谱 2.1 仪器 检测器。因其体积小、重量轻，具有理想的扫描线性、 采用CCD短波技术的INCE-9210MT近红外牛奶分 高分辨率和高光电灵敏度及大动态范围等优点，CCD检 析仪（北京英贤仪器