8万吨醋酸车间蒸馏岗位生产工艺设计方案.docVIP

摘 要 化学工业在我国发展十分迅速，而醋酸又是重要的化工原料及有机产品。本设计的主要设备是精馏塔，精馏设计包括方案的选取，主要设备的工艺条件的选取，主要设备的工艺设计计算——物料衡算、热量衡算、工艺参数的选定、设备的结构设计、工艺尺寸的计算、辅助设备的选型、工艺流程图的绘制等内容。 本设计针对醋酸精馏的问题进行分析、选取、计算、核算、绘图等，是较完整的精馏设计过程。设计过程中借助C语言求解精馏塔的泡、露点及相对挥发度，并运用了Excel表格等其它工具进行计算，通过设计计算得到了精馏塔的基本的设计尺寸，其操作弹性好，生产灵活，在工业生产中具有较大的可行性。 设计过程中用CAD绘制了氧化岗位的带控制点的工艺流程图及乙醛贮罐的配管图，并手工绘制了精馏工艺的车间设备布置图。 关键词：精馏；醋酸；工艺参数；操作弹性 Abstract The chemical industry in china has developed very quickly, and acetic acid is an important chemical materials and organic products. The design of the main equipment is distillation，Distillation design including the selection of programme，Major equipment selection process,Major equipment design and calculation process-material balance,heat balance,technical parameters of the selected,the structural design of equipment,size of the calculation,selection of auxiliary equipment,technological process of drawing, etc. This acetate designed for the distillation of the issues, select, computing, accounting, graphics, is a more complete design of the distillation process.The design process using C language distillation columns for the bubble, dew point，And use the Excel spreadsheet and other tools, Through the design of the distillation column calculated the size of the basic design,its operational flexibility, and production flexibility in industrial production in the greater feasibility. The design process using a CAD drawing of the posts with the control point plan and the process of acetaldehyde tank piping plans and hand-drawn distillation of the workshop equipment layout. Key word ： distillation acetic acid technical parameters operational flexibility 目 录 摘 要 I Abstract II 前 言 1 第1章 物料衡算 2 1.1设计基础 2 1.1.1原料、公用工程及产品规格 2 1.1.2塔出料情况 4 1.1.3其他工艺条件 4 1.2脱低沸物塔T0117和脱高沸物塔T0119的物料衡算 5 1.2.1流程示意图 5 1.2.2 脱低沸物塔T0117和脱高废物塔T0119的物料衡算 5 1.2.3循环锰组成计算 6 1.2.4 脱低塔顶排计算 6 1.2.5 脱低塔底排计算 7 1.2.6 脱高塔底排计算 7 1.2.7 物料衡算 7 第2章 塔的热量衡算 9 2.1 脱低塔T0117热量衡算 9 2.1.1流程示意图 9 2.1.2求解回流比 9 2.1.3设备热量衡算 10 2.3脱高沸物塔T0119热量衡算 11 2.3.1