APT和萃取复型研究压力容器模拟钢中富Cu团簇的析出.pdfVIP

47 3 Vol.47 No.3 2011 3 269—274 ACTA METALLURGICA SINICA Mar. 2011 pp.269–274 APT ℄ Cu ∗ 1) 1) 1) 2) 2) 1) 1) , 200072 2) , 200444  (APT) Cu . Cu 880 , 660 /10 h , 370 ,  APT 4500 h , Cu  3.1×1023 m−3 . Cu  1—5 nm ,  Cu . Ni Mn Cu  ,  .  4% 5 nm Cu  α–Fe , HRTEM EDS , Cu  ,  Cu 10%—80%() Cu–Fe(Ni, Mn) , 9R fcc ℄. , Cu , , , TG142.1 A 0412−1961(2011)03−0269−06 APT AND EXTRACTION REPLICA CHARACTERIZA- TION OF Cu–RICH CLUSTERS PRECIPITATED IN PRESSURE VESSEL MODEL STEELS CHU Dafeng 1), XU Gang 1), WANG Wei 1), PENG Jianchao 2), WANG Jun’an 2), ZHOU Bangxin 1) 1) Institute of Materials, Shanghai University, Shanghai 200072 2) The Key Laboratory for Advanced Micro–Analysis, Shanghai University, Shanghai 200444 Correspondent: ZHOU Bangxin, professor, Tel: (021 E-mail: zhoubx@shu.edu.cn Supported by National Basic Research Program of China (No.2006CB605003) and National Natural Science Foundation of China (No Manuscript received 2010–09–14, in revised form 2010–11–24 ABSTRACT The precipitation of Cu–rich clusters in reactor pressure vessel (RPV) model steel was investigated by means of atom probe tomography (APT), extraction replica (ER) and HRTEM. RPV model steel was prepared by vacuum induction furnace melting with higher content of Cu (0.6%, mass fraction). The ingot (about 50 kg of weight) was forged and hot–rolled to 4 mm in thickness and then cut to specimens of 40 mm ×30 mm. Those specimens were further heat