复方中药红外指纹图谱鉴定.pdfVIP

L ISH IZH EN MEDIC INE AND MATER IA MED ICA RESEARCH 2007 VOL. 18 NO. 6 2007 18 6 李湘南, 刘小平 (, 430070) : 寻找能够鉴定复方中药的新方法 利用傅立叶变换红外分 仪, 以复方板蓝根颗粒和六味地黄 丸为 例, 分别测试两种制剂与各自组方中缺不同药味制剂的红外光谱 两种复方中药与各自缺方制剂的无水乙醇提取 物的红外图谱峰强和峰位存在差异, 但是光靠人工比较难以得出正确结论, 通过相似度计算可以得到比较客观的结果 傅立叶变换红外图谱定量分 法可用于复方中药的鉴定 : 复方中药; 复方板蓝根颗粒; 六味地黄 丸; 傅立叶变换红外光谱 : R282. 5 : A : 2007) Iden tification of Compound Ch inese D rug by FT IR Sp ectrum LIX iangnan, LIU X iaoping (C olleg e of Chem icalE ng ineering , Wuhan Un iv ers ity of Tech nology , Wuhan 430070, Ch ina ) Abstract: O bjective T o de elop a new m ethod of identify ing Ch inese drug. M ethods U sing Foru ier transform infrared ( FT IR) spectrom etry , compound radix isatidis granu les, Liu W ei DiH uangW an and each incom plete form ula preparation w ere determ ined. R esu ts Peak intensity and wa enum ber of the FT IR spectra were d ifferen t. The exact conclusion was difficult to drawn only by m anual work, and the objecti e conclusion was drawn by smi ilarity calculation . Conc u sion FT IR technology can be used for the identification of Com pound Chinese Drug. K ey w ord s: Compound Ch inese drug; Radix isat id is g ranules; L iuW ei DHi uangW an; FT IR spectra [6] , 2. 1. 3 六味地黄 丸全样的制备 , , 2005! 40 1 , , 100, 5 , , 2. 1. 4 六味地黄 丸缺方样品的制备 [ 1~ 4] , , , , 100 FT IR , 12, 13, 14, 15 , , 2. 2 方法 , 2. 2. 1 样品测定 1~ 15 0. 1 g , , , 5 m l, 20 m in, 1~ 15 1 2 g , 1~ 15 1. 1 仪器 W QF200 ( 3, 1 - 1 , 4 400~ 400 cm , 16, 4 cm ; , KQ100B( ); 2. 2. 2 精密度实验 1 5, 1. 2 药