惰性气体雾化法制备Fe-Si-Al-Ni-Ti软磁合金粉末.pdfVIP

I39惰性气体雾化法制备Fe-Si-Al-Ni-Ti 软磁合金粉末 刘辛谢焕文蔡一湘骆接文王蕾 （广州有色金属研究院 粉末冶金研究所，广州 510651） Fe-3%Si-0.5%Al-2%Ni-2%Ti X 摘要：采用惰性气体雾化法制备 软磁合金粉末，通过化学分析、 射线衍射仪、激光粒度 分析仪、电子探针等手段分别对粉末的成分、物相结构、粒度分布、表面形貌和截面组织进行表征，研究雾化压力和 雾化温度对粉末粒径和形貌的影响。结果表明：当雾化压力为 5.5 MPa、雾化温度为 1550 ℃时，粉末中值粒径为 54.38 μm ，颗粒表面粗糙且球形度不高；当雾化温度为 1550 ℃、雾化压力由 5.5 MPa 增大至 6.5 MPa 时，粉末中值粒径由 54.38 μm 减小至 35.51 μm ，颗粒表面卫星粉末增多；当雾化压力为 5.5 MPa、雾化温度由 1550 ℃提高至 1650 ℃时， 粉末中值粒径由 54.38 μm 减小至 36.63 μm ，粉末表面光滑且球形度增大；粉末的物相结构为单一的α-Fe 相，粉末内部 组织形态主要是等轴晶，并伴有少量枝晶。 关键词：气雾化；Fe-Si-Al-Ni-Ti ；软磁合金粉末 Fe-Si-Al-Ni-Ti soft magnetic alloy powder prepared by inert-gas atomization LIU Xin, XIE Huanwen, CAI Yixiang, LUO Jiewen, WANG Lei (Department of Powder Metallurgy, Guangzhou Research Institute of Non-ferrous Metals, Guangzhou, 510651, China) Abstract: Fe-3%Si-0.5%Al-2%Ni-2%Ti soft magnetic alloy powders were prepared by inert-gas atomization. The composition, phase structure, size distribution, surface morphology and cross-sectional microstructure of the powder were characterized by chemical analysis, X-ray diffractormeter, laser scattering particle size distribution analyzer and electron probe microanalyzer, respectively. The effects of gas atomization pressure and temperature on the powder size and morphologies were also investigated. The results indicate that when the gas atomization pressure is 5.5 MPa and the temperature is 1550 ℃, the median diameter of the powder, which appears rough surface and low sphericity, is 54.38 μm. When the gas atomization temperature is 1550 ℃, with the gas atomization pressure i