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SC-1997-701-酯交换制备环亚硫酸酯.pdf
SYNTHETIC COMMUNICATIONS, 27(4), 701-707 (1997)
PREPARATION OF CYCLIC SULFITES BY TRANSESTERIFICATION
OF DIOLS AND DIISOPROPYL SULFITE
Steven A. King,* Brenda Pipik,* David A. Conlon and M. Bhupathy
Department of Process Resear, Merck Research Laboratories
R80Y-355, P.O.Box 2000, Rahway, NJ 07065-0900,USA
Abstract: Cyclic Sulfites of 1.2-, 1,3- and 14-diols canbe prepared in high yield by acid or base
catalyzed transesterificationwith diisopropyl sulfite.
Cyclic sulfites of 1.2- and 1.3- diols have s
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