拟除虫菊酯类农药残留检测前处理技术研究进展.pdfVIP

第49卷第1期 农 药 Vol. 49, No. 1 2010年1月 AGROCHEMICALS Jan. 2010 综述 拟除虫菊酯类农药残留检测前处理技术研究进展 孙成玲，汪付星，颜冬云，徐绍辉 (青岛大学 化学化工与环境学院， 山东 青岛 266071) 摘要： 拟除虫菊酯农残检测前处理技术是制约其分析速度和分析准确度的瓶颈。 综述最近几年应用于拟除虫 菊酯类农药残留检测前处理技术如萃取技术(包括超临界流体萃取、加速溶剂萃取、超声波萃取、微波辅助萃取 和液相微萃取等)、净化技术(包括凝胶渗透色谱和固相萃取等)以及基于固相微萃取和基质固相分散萃取等萃 取、净化一体化技术的国内外研究进展，为我国更好的开展农残检测工作提供理论依据与技术支撑，并对其发 展趋势进行了展望。 关键词： 拟除虫菊酯；样品前处理技术；展望 中图分类号： 文献标志码： 文章编号： TQ450.2 A 1006-0413(2010)01-0011-05 Progress on the Research of Sample Pretreatment Techniques in the Detection of Pyrethroid Residues SUN Cheng-ling, WANG Fu-xing, YAN Dong-yun, XU Shao-hui (College of Chemical Engineering and Environmental Sciences, Qingdao University, Qingdao 266071, Shandong, China) Abstract: Sample pretreatment techniques in the detection of pyrethroid residues have been the bottleneck of restricting its analysis speed and accuracy. The recent progresses on the studies of pretreatment techniques in the detection of pyrethroid residues were reviewed. The methods described consist of extraction techniques which include supercritical fluid extraction, accelerated solvent extraction, ultrasonic extraction, microwave-assisted extraction and liquid-phase micro-extraction; purifi cation techniques which include gel permeation chromatography and solid-phase extraction, and integration techniques based on solid-phase micro-extraction and matrix solid-phase dispersion extraction. A theoretical basis and technical support were provided for our country to carry out better