La-Ca-Sr-Co系高性能干压各向异性永磁铁氧体的研制.pdfVIP

工艺·技术·应用 La-Ca-Sr-Co 系高性能干压各向异性永磁铁氧体的研制 王颖泉，滕阳民，王常蕾，王 倩 （北矿磁材科技股份有限公司，北京 100070 ） 摘 要：以北矿 BMS-12 预烧料为基料，首先通过湿压工艺确定出适宜的二次添加剂添加量，在此基础上 采用干压法制备各向异性永磁铁氧体材料，分析黏合剂、润滑剂用量及磁粉粒度对磁体性能的影响。实验结果 表明，樟脑黏合剂和硬脂酸钙润滑剂的适宜添加量分别为 0.6wt% 、0.8wt%。在 0.85~1.00μm 的粉料粒度范围内 都可以获得较高的剩磁和矫顽力。得到的典型干压磁体性能：Br=421mT, Hcb=296kA/m, Hcj=360kA/m, (BH) 3 max=33.2kJ/m ，达到 TDK 的 FB5D 性能水平。La-Ca-Sr-Co 系干压磁体具有比传统锶永磁铁氧体湿压磁体 更高的剩磁和内禀矫顽力。 关键词：永磁铁氧体；干压成型；添加剂；粉料粒度；磁性能 中图分类号：TM277+ .5 文献标识码：A 文章编号：1001-3830(2015)01-0036-04 Development of high performance La-Ca-Sr-Co system dry-press anisotropic permanent ferrite WANG Ying-quan, TENG Yang-min, WANG Chang-lei, WANG Qian BGRIMM Magnetic MaterialsTechnology Co, Ltd, Beijing 100070, China Abstract ：Based on BMS-12 pre-sintered ferrite powders, suitable amount of additives is determined through the wet-pressing process. On this basis, dry-pressed anisotropic permanent ferrite material was prepared and effects of adhesives, lubricants dosage and powder size on magnetic properties analysized. The experimental results show that, the appropriate amount of camphor adhesive and calcium stearate lubricant is 0.6wt% and 0.8wt%, respectively. High remanence and coercivity can be obtained for particle size of 0.85 to 1.00 μm. Dry-pressed magnet ferrite was prepared 3 with typical properities of Br=421mT, Hcb=296kA/m, Hcj=360kA/m, (BH)max=33.2kJ/m , reaching the level of TDK FB5D. Dry-pressed magnet of La-Ca-Sr-Co system has higher remanence and intrinsic coercivity than traditional we