磷化工艺制备绝缘软磁粉末及其频率特性研究.pdfVIP

20 5 Vol. 20 No . 5 2010 10 POWDER METALLURGY INDUSTRY Oct . 2010 1, 2 1 1 1 1 , , , , ( 1 , 271109; 2 , 100083) : 经绝缘处理的软磁粉末在高频( 1 kHz) 下具有良好的频率特性和较低的磁损耗 本文以还原 铁粉为研究对象, 采用磷化处理工艺制备绝缘软磁粉末, 并分析了其频率特性 研究结果显示: 经磷化处理和充分洗涤获得的粉末颗粒, 其频率特性得到明显改善, 即高频磁 损耗降低振幅磁导率随频率变化波动变小400退火处理使粉末颗粒表面变得光滑且内部 孔隙减少, 再经磷化处理, 高频磁损耗进一步降低, 250kHz 下的磁损耗是 铁粉的407%, 是 单 一磷化处理铁粉的703%; 振幅磁导率提高, 在( 10~ 250) kHz 下其值保持在92 以上经 EM 和ED 分析, 绝缘粉末颗粒表面被05~ 1 m 厚度的磷酸铁盐包覆 : 绝缘软磁粉末; 还原铁粉; 磷化; 退火处理; 频率特性 : TF 123; TM271 : A : 1006- 6543( 2010) 05- 0023- 04 FREQUENCY CHARACTERI T IC OF IN ULAT ED OFT MAGNET IC POWDER BY PHO PHAT IZAT ION PROCE 1, 2 1 1 1 1 TIAN Jian-jun , CUI Jian-min ,YUAN Yong , Z ANGDe-jin , LI Ting ( 1Lai Wu Iron teel Group Pow der Metallurgy Co LTD, Laiw u, 271109, China, 2Universit y of cience and Technology Beijing, Beijing, 100083, China) Abstract: oft magnetic pow der by insulating process had excellent frequency characteristic and low magnetic loss in higher frequency ( 1kHz)Insulated soft magnetic powder had been prepared by phosphatization process using reduction iron pow der in this pa- perFrequency characteristics of the pow der had been studiedT he results indicated that the frequency characteristics of the pow der w ere improved by phosphatization processT he mag- netic loss decreased and the stability of amplitude permeability increasedWhen the pow der w as annealing heat treated at 400 before the phosphatiation process, surface of th