Analytical Method for Estimation of a New Insecticide Flubendiamide and its Safety Evaluation for Us.pdfVIP

Bull Environ Contam Toxicol (2008) 81:360–364 DOI 10.1007/s00128-008-9470-1 Analytical Method for Estimation of a New Insecticide Flubendiamide and its Safety Evaluation for Usage in Rice Crop Madhuban Gopal Æ Ekta Mishra Received: 6 October 2007 / Accepted: 14 May 2008 / Published online: 28 June 2008 Springer Science+Business Media, LLC 2008 Abstract The paper presents a method for residue anal- It has larvicidal activity as a stomach poison and is an oral ysis of flubendiamide in rice (Oryza sativa), which includes intoxicant, fast acting (rapid cessation of feeding), long improved extraction, cleanup and determination of flu- lasting (rain fast) and has limited plant penetration and bendiamide in rice seeds, husk and straw by using LC with systemicity. It has a novel biochemical action as it affects UV detection. Safety evaluation of this insecticide in rice calcium ion balance irrespective of sodium or potassium has been carried out after applying its soluble concentrate ion balance (Hall et al. 1995), which causes contraction of (SC) formulation at recommended dose (30 g a.i. ha-1) insect skeletal muscle (Usherwood 1962). and double of the recommended dose (60 g a.i. ha-1) on Flubendiamide has been used in plant protection as a new rice crop. MRL of flubendiamide on rice grain can be agricultural material for productivity improvement demon- proposed as 0.2 mg kg-1. stration test and for noxious insect prevention measure test with chemical pest control in Japan (Tohnishi et al. 2005b). Keywords Flubendiamide Rice (Oryza sativa) The persistence study of flubendiamide and its metabolite Residue analysis MRL