《Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics》.pdfVIP

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《Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics》.pdf

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Journal of Wuhan University of Technolotgy-Mater. Sci. Ed. Dec. 2008 883 DOI 10.1007/s11595-008-6883-y Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics LIU Jun, OU Yang, XU Changwei, QI Hong (Materials Science and Engineering School, Shenyang Jianzhu University, Shenyang 110168,China) Abstract : A Cao-Mgo-Al O -SiO quaternary system was established with the main crystal 2 3 2 phase design based on Diopside, and the effect of once-through sintering heat treatment on micro- structure of iron tailings glass ceramics was studied by using DTA, SEM along with measurement of microhardness and volume density. The experimental results show that, when the total amount of FeO and Fe O exceeds 10wt%, a large number of fine nuclei are produced in the annealing process, 2 3 and the phenomenon of nucleus resorption happens during the process of nucleation heat treatment, which is unfavorable for preparing iron tailings glass ceramics through once-through sintering method. When the annealing temperature from 1250 ℃ to 830 ℃, setting crystallization time for 4h, without heat treatment, crystals are well grown with arrangement and interlocking in glass phase. At 830 ℃ the crystals a