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Effect of anions during hydrothermal preparation of boehmites.pdf

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Effect of anions during hydrothermal preparation of boehmites

March 2002 Materials Letters 53 Ž2002. 133–137 rlocatermatlet Effect of anions during hydrothermal preparation of boehmites a a, ) b a D. Mishra , S. Anand , R.K. Panda , R.P. Das a ( ) Regional Research Laboratory CSIR , Hydro and Electro Metallurgy DiÕision, Bhubaneswar, 751 013, Orissa, India b Berhampur UniÕersity, Berhampur, 760 007, Orissa, India Received 7 December 2000; received in revised form 24 June 2001; accepted 25 June 2001 Abstract Boehmites were precipitated hydrothermally from different inorganic aluminum salt solutions under similar conditions using urea as the precipitating agent. It was observed that the hydrolysis of Al 2ŽSO4 .3 starts at a lower temperature due to Ž . Ž . formation of hydroxy sulfates in comparison to AlCl3 and Al NO3 3 solutions. The boehmite obtained from Al2 SO4 3 has a Ž . lower water content, and a higher surface area than the boehmites obtained either from AlCl 3 or Al NO3 3. The boehmite obtained from Al2ŽSO4 .3 was lighter giving lower tap density value. Depending on the nature of anion present during synthes