《Lowtemperature electrochemical synthesis and characterization of ultrafine YOH3 and Y2O3 nanoparticles》.pdfVIP
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Availableonlineatwww.sciencedirect.corn
.一,,
峰::,ScienceDirect
JOURNALOFRARE
登一 EARTHS,VoL30。No.3。Mar.2012,P.236
electrochemicalandcharacterizationofultrafine‘
Low—temperature synthesis
and
Y203
Y(OH)3 nanoparticles
Mustafa GHAEMl3
AGHAZADEHl,TaherYOUSEFl2,Mehdi
flLaser
oBox49138-15739
Chem西try,ScienceFaculty,GolestanUniversity,P Gorgan.1ran)
Received28March201 1 1 2011
l;revisedSeptember
fromall 0.005moI/L bathonthe
Abstract:UltrafineY(0Hk were additive—free YCl3
nanoparticlessuccessfullydeposited low-temperature
of at600
steelcathodeatthecurrent of0.5mm/cm2andbath 10oC.Heattreatmentofthe Y(0Hk
density temperature prepared nanoparticles
of
oCinair1edtotheformationofY,01 behaviorand transformationtheheattreatment were
nanoparticles.Thermalphase during Y(OHk
differential structuresand
calorimetry(DSC)andthermogramimetricanalysis(TGA).Themorphologies,crystal
investigatedby scanning
ofthe materialswereexaminedmeansof andtransmissionelectron andTEM)aswell
compositionsprepared by scanning microscopy(SEM
as FT—IR resultsshowedthatthe was
X.raydiffractionⅨRD)andspectroscopy.The preparedY(OH)3nanoparticlesessentiallyamorphous
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