《Li4Ti5O12 36种合成方法汇编》.pdfVIP

Li4Ti5O12 合成方法汇编 1 The Li –Ti –O ternary phase was prepared by two meth- ods. The first was the conventional method_method A. which is heating a mixture of TiO anastase and Li Co at 2 2 3 8008 for 12 h in a nitrogen gas stream. The second method _method B.used was high energy ball milling _HEBM. ofprecursor to form nanocrystalline phases. These materials were then heat treated in order to obtain the desired phases. 2 2.1. Sample preparations 2.1.1. AA-assisted sol –gel method (A) This method involves the