原创力文档《Synthesis under Microwave Irradiation and Crystal Structure of 4-(3,4-Methylenedioxylphenyl)-6-methyl- 5-ethoxycaronyl-3,4-dihydropyrimidin-2(H)-one》.pdfVIP
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《Synthesis under Microwave Irradiation and Crystal Structure of 4-(3,4-Methylenedioxylphenyl)-6-methyl- 5-ethoxycaronyl-3,4-dihydropyrimidin-2(H)-one》.pdf
23 卷5 期 结 构 化 学 JIEGOU HUAXUE Vol. 23, No. 5
2004. 5 Chinese J. Struct. Chem. 494~497
Synthesis under Microwave Irradiation and Crystal
Structure of 4-(3,4-Methylenedioxylphenyl)-6-methyl-
5-ethoxycaronyl-3,4-dihydropyrimidin-2(H)-one
TU Shu-Jiang FANG Fang JIANG Hong ZHU Song-Lei
LI Tuan-Jie ZHANG Xiao-Jing SHI Da-Qing
(Department of Chemistry, Xuzhou Normal University; Key Laboratory of
Biotechnology on Medical Plant of Jiangsu Province, Xuzhou, Jiangsu 221009, China)
ABSTRACT The title compound 4-(3,4-methylenedioxylphenyl)-6-methyl-5-ethoxycaronyl-3,4-
dihydropyrimidin-2(H)-one (C H N O ) has been synthesized and determined by single-crystal
15 16 2 5
X-ray diffraction. The crystal is of triclinic, space group with a = 7.580(1), b = 7.920(2), c =
13.168(4) Å, a = 96.44(2), b = 96.71(2), g = 109.81(2), V = 728.8(3) Å3, Z = 2, M = 304.30, D =
r c
3 1
1.387 g/cm , F(000) = 320, m(MoKa) = 0.105 mm (l = 0.71073 Å), R = 0.0446 and wR = 0.1205.
In the molecule the pyrimidine ring adopts a boat conformation.
Keywords: microwave irradiation, 3,4-dihydropyrimidinone, toluene-p -sulfonic acid (TsOH),
crystal structure
1 INTRODUCTION
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