PZN-PZT压电陶瓷流延膜的制备.docx

 PAGE - 2 - 分 数：评卷人： 研究生《电子技术综合实验》课程论文 题 目：流延膜的制备 学 号 姓 名 专 业 指 导 教 师 院（系、所） 年 月 日  七选一实验  PAGE - 15 - 七选一实验 摘 要 多层压电陶瓷具有低压驱动、薄型化、高功率密度等优点,拥有广泛的应用前景。其中共烧多层压电陶瓷更是将陶瓷层和电极层构成的器件整体进行烧结，相对于分别烧结后粘接等其他方法而言,这种方法所得器件具有更高的整体性能和使用稳定性[1]。 目前对于多层压电陶瓷的研究多在陶瓷的制备和性质方面,但与应用背景结合紧密的研究比较缺乏，而本文重点研究压电陶瓷流延法制膜。 通过分析各种有机添加剂在流延浆料中的作用机理与选择原则，并根据本文需要，选定分散剂为三油酸甘油酯，粘合剂为聚乙烯醇缩丁醛（PVB），溶剂为丁酮和乙醇组成的二元混合有机溶剂，增塑剂为聚乙二醇 400和聚乙二醇 2000。实验研究制备 PZN-PZT 系压电陶瓷的流延膜片，探讨不同配比的粘合剂和不同的固含量对流延浆料和流延膜片性能的影响，并最终确定一个最优的配比方案。 关键词：压电陶瓷； PZN-PZT 材料；有机添加剂；流延 Abstract The piezoelectric ceramic materials of Pb (Zr, Ti) O3 (PZT) have been widely used for numerous of applications such as actuators and transformers because of their excellent piezoelectric properties. Recently, multilayer piezoelectric ceramic devices have been widely investigated and applied, which can be driven under a low voltage and a low power than conventional piezoelectric ceramic devices. [1] Nowadays, the researches on the piezoelectric ceramic materials are mainly on its preparation or the properties, but only a few of researches are based on the ceramic-materials. Though discussing the organic additives’ mechanism, selective rules and their roles in preparing tape-casting ceramic slurry and according to the characteristic of our experiment, triolein is chosen as dispersant, polyvinyl butyral (PVB) is chosen as binder, polyethylene glycol (PEG) 400 and PEG2000 are chosen as plasticizer, and butanone with ethanol are chosen as dual-combining solvent. Keywords: piezoelectric ceramic; PZN-PZT; organic additives’ mechanism; tape casting 目 录 TOC \o 1-3 \h \u  HYPERLINK \l _Toc343869236 摘 要  PAGEREF _Toc343869236 \h - 2 -  HYPERLINK \l _Toc343869237 Abstract  PAGEREF _Toc343869237 \h - 3 -  HYPERLINK \l _Toc343869238 第1章 绪论  PAGEREF _Toc34