氧化铝生产控制分析.doc

目录 第一章生料浆制备··················· 1.1 试样的采取··························· 1.1.1 铝矿石和石灰石的取样···················· 1.1.2 原煤的取样························· 1.1.3 焦炭的采样························· 1.1.4 纯碱的取样························· 1.1.5 氧化铝及其氢氧化铝的取样·················· 1.1.6 铝酸钠浆液的取样······················ 1.2 分析试样的制备························· 1.2.1 原料的烘干························· 1.2.2 试样的破碎························· 1.2.3 样品的过筛························· 1.2.4 样品的混匀························· 1.2.5 样品的缩分························· 1.2.6 铝矿石、石灰石、焦炭及熟料的试样处理············ 1.2.7 矿浆、赤泥试样处理····················· 1.2.8 生料浆试样处理······················· 1.2.9 氧化铝及氢氧化铝试样处理·················· 1.2.10 铝酸钠溶液的制备····················· 第二章 试剂的配制························ 2.1 试剂浓度的表示方法······················· 2.1.1 百分浓度（%）······················· 2.1.2 体积比（V：V）······················· 2.1.3 当量浓度（N）······················· 2.1.4 摩尔浓度（M）······················· 2.1.5 滴定度（T）························ 2.2 标准溶液的配制和标定······················ 2.2.1 标准溶液的配制方法····················· 2.2.2 标准溶液标定的方法····················· 2.2.3 标准溶液的调整······················· 2.3 酸、碱、EDTA及硝酸锌标准溶液的配制和标定··········· 2.3.1 标准碱液的配制和标定···················· 2.3.2 标准酸液的配制和标定···················· 2.3.3 锌标准溶液的配制······················ 2.3.4 EDTA标准液的配制和标定··················· 2.4 其它标准溶液的配制和标定···················· 2.4.1 0.1N草酸钠标准液······················ 2.4.2 0.1N高锰酸钾标准液····················· 2.4.3 0.1N氯化钠标准液······················ 2.4.4 0.1N硝酸银标准液······················ 2.4.5 0.1N硫氧化铵标准液····················· 2.5 比色分析标准溶液的配制····················· 2.5.1 二氧化硅标准液的配制···················· 2.5.2 三氧化二铁标准液的配制··················· 2.5.3 二氧化钛标准液的配制···················· 2.5.4 氧化钠、氧化钾标准液的配制················· 2.5.5 三氧化二镓标准液······················ 2.6 常用试剂的配制·························· 2.6.1 常用指示剂的配制······················ 2.6.2 主要常用试剂的配制····················· 第三章 铝矿石的分析······················· 3.1 二氧化硅的测定························· 3.1.1 方法概述···········