常用标准溶液配及标定.docVIP

氢氧化钠标准溶液 制备 在陶瓷容器内将氢氧化钠和水按等质量配成浓碱溶液，冷却后转入塑料容器中，密闭放置1～2月至溶液清亮，按下表规定体积吸取上层清液，用不含二氧化碳的水稀释至1000ml，摇匀，密闭放置10d，将上层溶液虹吸入另一清洁的硬质玻璃瓶内，摇匀以备标定。 C（NaOH））））(SO4)2]=m/[(V-V0)*0.049032] 式中: C(FeSO4)—硫酸亚铁标准溶液的物质的量浓度,mol/L C[(NH4)2Fe(SO4)2] —硫酸亚铁铵标准溶液的物质的量浓度mol/L m—重铬酸钾的质量,g V —硫酸亚铁(或硫酸亚铁铵)溶液的用量,ml V0—空白试验硫酸亚铁(或硫酸亚铁铵)溶液的用量,ml 高锰酸钾法 方法提要：以高锰酸钾标准溶液为基准物,在酸性溶液中与亚铁反应 试剂：高锰酸钾标准溶液[C (1/5KMnO4)=0.1mol/L] 分析步骤 吸取20.00-30.00ml硫酸亚铁(或硫酸亚铁铵)溶液于250ml锥形瓶中,加50ml沸水并已冷却的水,在不断摇动下,以高锰酸钾标准溶液滴至溶液呈粉红色保持30s不消失为终点. 计算 C(FeSO4)或C [(NH4)2Fe(SO4)2]=C1*V1/V 式中: C(FeSO4)—硫酸亚铁标准溶液的物质的量浓度,mol/L C[(NH4)2Fe(SO4)2] —硫酸亚铁铵标准溶液的物质的量浓度mol/L V1—重铬酸钾标准溶液的物质的量浓度,mol/L V —硫酸亚铁(或硫酸亚铁铵)溶液的用量,ml the real implementation of the quasi, ruthless. Tough, requirement, carry forward the spirit of a nail, and the corrective measures The implementation of the nerve endings, do not let the rectification is not in place, not to retreat, the people are not satisfied. Pin four is to adhere to the reform and innovation. To reform the way of thinking and innovative courage to turn style, against four winds, the courage to face the contradictions, good at solving the chronic ills, dare to break the outdated customs and bad habits Hensha unhealthy tendencies, trees, fresh healthy. The five is to adhere to tackling the problem. That is the wind Su Ji and the education supervision combined, in order to establish a new system to promote the normalization of style building, long-term, to enhance the party spirit of honest and pragmatic people thought conscious action. The six is to insist on the completion of the third grasp the overall situation. Activity and end This year the goal of safety production work plan for next year, work together, to promote the activities and the work of production safety with both hands, two promotion, two not mistake. Two, rectification of the overall objectives and specific objectives: (a) the overall path around the four focus, carried out the outstanding problems of the special rect