牡蛎钙英文检方OYSTER 40.docVIP

CALCIUM CARBONATE OYSTER 40% IDENTIFICATION It gives the reaction of carbonates 2.3.1 . weighs approximately 100 mg of sample and transfer to a test-tube of 20ml add 2ml of purified water and stirring until a suspension add 3 ml of dilute acetic acid solution, and Close the tube immediately using a stopper fitted with a glass tube bent twice at right angles. the solution must become effervescent and gives off a colourless and odourless gas. Heat gently and collect the gas in 5 ml of barium hydroxide solution A white precipitate is formed that dissolves on addition of an excess of hydrochlori